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Beilstein J. Org. Chem. 2014, 10, 2654–2657, doi:10.3762/bjoc.10.278
Graphical Abstract
Figure 1: Targeted modified cyclodextrins.
Scheme 1: Synthesis of bicatenar CDs 4, 5, 6 and 7; a) succinic anhydride, 135 °C, 10 min, 70%; b) phytosphin...
Beilstein J. Org. Chem. 2014, 10, 2642–2648, doi:10.3762/bjoc.10.276
Scheme 1: Synthesis of CD-substituted polymers 3a, 3b and 3c.
Figure 1: 1H NMR spectrum of 3c in D2O at 25 °C.
Figure 2: 31P NMR spectrum of 3b in a) DMF-d7 at 25 °C and b) D2O at 25 °C.
Figure 3: 1H NMR spectrum of 3b (10 mM) in D2O at 25 °C (below) and 60 °C (above).
Figure 4: Size-exclusion chromatography of polyNAS and polymers 3a, 3b and 3c.